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Novel nanocarbons via facile one-pot combustion synthesis

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dc.abstract.enCarbon nanomaterials like fullerenes, nanotubes and graphene are of great interest for the current research as well as for industrial applications. Herein a novel and facile protocol for the fast and autothermal formation of different types of nanocarbons including 3 D graphene-like nanosystem via combustion synthesis is presented. Magnesiothermic reduction of carbon-bearing oxidants (both pure chemical reagent and consumer commodities) resulted in their total conversion yielding solid raw products containing mostly nanocrystalline magnesium oxide, porous carbon and layered graphene-related nanomaterial. The combustion reaction was also optically online monitored to follow the reaction course. Purification in mineral acid removed the as-formed MgO and the non-reacted reducer and hence enabled the efficient recovery of the carbon product. The reactants and products were characterized using electron microscopy, X-ray diffraction and Raman spectroscopy. Chemical composition was probed by EDS and elemental analysis. The adsorption performance of purified products was also evaluated.
dc.affiliationUniwersytet Warszawski
dc.contributor.authorFronczak, Maciej
dc.contributor.authorBogati, Rabi Sharan
dc.contributor.authorPandey, Manoj
dc.contributor.authorSubedi, Deepak Prasad
dc.contributor.authorTiwari, Santosh K.
dc.contributor.authorKafle, Bhim
dc.contributor.authorBaranowski, P.
dc.contributor.authorDąbrowska, Agnieszka
dc.contributor.authorHuczko, Andrzej
dc.contributor.authorBystrzejewski, Michał
dc.contributor.authorDobrzycki, Łukasz
dc.date.accessioned2024-01-25T13:52:28Z
dc.date.available2024-01-25T13:52:28Z
dc.date.issued2022
dc.description.financePublikacja bezkosztowa
dc.description.volume121
dc.identifier.doi10.1016/J.DIAMOND.2021.108746
dc.identifier.issn0925-9635
dc.identifier.urihttps://repozytorium.uw.edu.pl//handle/item/113960
dc.identifier.weblinkhttps://api.elsevier.com/content/article/PII:S0925963521005094?httpAccept=text/xml
dc.languageeng
dc.pbn.affiliationchemical sciences
dc.relation.ispartofDiamond and Related Materials
dc.relation.pages108746
dc.rightsClosedAccess
dc.sciencecloudnosend
dc.subject.enNanocarbon
dc.subject.enCombustion synthesis
dc.subject.enMagnesiothermic reduction
dc.subject.enSurface morphology
dc.titleNovel nanocarbons via facile one-pot combustion synthesis
dc.typeJournalArticle
dspace.entity.typePublication