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WO3 Nanopores Array Modified by Au Trisoctahedral NPs: Formation, Characterization and SERS Application

dc.abstract.enThe WO3 nanopores array was obtained by an anodization method in aqueous solution with addition of F- ions. Several factors affecting the final morphology of the samples were tested such as potential, time, and F- concentrations. The morphology of the formed nanopores arrays was examined by SEM microscopy. It was found that the optimal time of anodization process is in the range of 0.5–1 h. The nanopores size increased with the increasing potential. The XPS measurements do not show any contamination by F- on the surface, which is common for WOx samples formed by an anodization method. Such a layer was successfully modified by anisotropic gold trisoctahedral NPs of various sizes. The Au NPs were obtained by seed-mediated growth method. The shape and size of Au NPs was analysed by TEM microscopy and optical properties by UV-VIS spectroscopy. It was found that the WO3-Au platform has excellent SERS activity. The R6G molecules could be detected even in the range of 10−9 M.
dc.affiliationUniwersytet Warszawski
dc.contributor.authorDziubałtowska, Małgorzata
dc.contributor.authorTurczyniak-Surdacka, Sylwia
dc.contributor.authorAmbroziak, Robert
dc.contributor.authorKrajczewski, Jan
dc.date.accessioned2024-01-23T07:21:55Z
dc.date.available2024-01-23T07:21:55Z
dc.date.copyright2022-12-06
dc.date.issued2022
dc.description.accesstimeAT_PUBLICATION
dc.description.financePublikacja bezkosztowa
dc.description.number23
dc.description.versionFINAL_PUBLISHED
dc.description.volume15
dc.identifier.doi10.3390/MA15238706
dc.identifier.issn1996-1944
dc.identifier.urihttps://repozytorium.uw.edu.pl//handle/item/125168
dc.identifier.weblinkhttps://www.mdpi.com/1996-1944/15/23/8706/pdf
dc.languageeng
dc.pbn.affiliationchemical sciences
dc.relation.ispartofMaterials
dc.relation.pages8706
dc.rightsCC-BY
dc.sciencecloudnosend
dc.subject.enanodization
dc.subject.enAu TOH NPs
dc.subject.enplasmonics
dc.subject.enSERS
dc.subject.enWO3 nanostructures
dc.titleWO3 Nanopores Array Modified by Au Trisoctahedral NPs: Formation, Characterization and SERS Application
dc.typeJournalArticle
dspace.entity.typePublication