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The assignment of 11B and 1H resonances in the post-reaction mixture from the dry synthesis of Li(BH3NH2BH2NH2BH3)

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cris.lastimport.scopus2024-02-12T19:32:42Z
dc.abstract.enWe report a detailed (Formula presented.) NMR and (Formula presented.) NMR study of as synthesised (Formula presented.) obtained in a novel dry-synthesis method. A combination of 1D and 2D single- and triple-quantum techniques was used for the assignment of all observed signals. Minor side-products and reactants were detected in the product: (Formula presented.), (Formula presented.), (Formula presented.), and two yet unknown salts containing 7-membered chain anions: (Formula presented.) and (Formula presented.). We believe the assignment provided within this study might be helpful when analysing the mixtures containing numerous ammonia borane derivatives, which often give overlapping signals that are hard to distinguish
dc.affiliationUniwersytet Warszawski
dc.contributor.authorKazimierczuk, Krzysztof
dc.contributor.authorKoźmiński, Wiktor
dc.contributor.authorOwarzany, Rafał
dc.contributor.authorPrus, Agnieszka
dc.contributor.authorNawrocka, Ewa K.
dc.contributor.authorFijałkowski, Karol
dc.date.accessioned2024-01-26T09:55:04Z
dc.date.available2024-01-26T09:55:04Z
dc.date.issued2023
dc.description.financePublikacja bezkosztowa
dc.description.number1
dc.description.volume61
dc.identifier.doi10.1002/MRC.5309
dc.identifier.issn0749-1581
dc.identifier.urihttps://repozytorium.uw.edu.pl//handle/item/121902
dc.identifier.weblinkhttps://onlinelibrary.wiley.com/doi/pdf/10.1002/mrc.5309
dc.languageeng
dc.pbn.affiliationchemical sciences
dc.relation.ispartofMagnetic Resonance in Chemistry
dc.relation.pages49-54
dc.rightsClosedAccess
dc.sciencecloudnosend
dc.subject.en11B NMR
dc.subject.en1H NMR
dc.subject.enamidoboranes
dc.subject.enammonia borane
dc.subject.enLi(B3N2)
dc.titleThe assignment of 11B and 1H resonances in the post-reaction mixture from the dry synthesis of Li(BH3NH2BH2NH2BH3)
dc.typeJournalArticle
dspace.entity.typePublication